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WebThe proposed catalyst loading, that is the ratio by volume of catalyst to aniline, is to be 0.03. Under the conditions of agitation to be used, it is estimated that the gas volume fraction in the three-phase system will be 0.15 and that the volumetric gas- liquid mass transfer coefficient (also with respect to unit volume of the whole three ... WebNov 19, 2024 · Catalytic reactions that use metal complexes as substrates, rather than catalysts, are nearly unknown. We recently demonstrated that certain flavins (FLs) are potent redox photocatalysts capable of converting PtIV anticancer prodrug complexes into PtII drugs in the biological environment. Herein, we investigate the mechanism of these … First, four sets of experiments were performed for AQE optimisation and the detailed conditions were presented in Supplementary Fig. 1. The AQE results of CuSA-TiO2 under different wavelength light irradiation (365 nm, 385 nm, 420 nm, and 520 nm) are shown in Supplementary Fig. 1a. It indicates a decrease with … See more To explore the science behind the outstanding photocatalytic performance of 1.5 wt% CuSA-TiO2 (named CuSA-TiO2 subsequently), a series of studies were performed. Firstly, the X-ray diffraction (XRD) patterns of the … See more To further confirm the charge dynamics of the excited TiO2 and CuSA-TiO2, the femto second transient absorption spectra (fs-TAS) were monitored and shown in Supplementary Fig. 19 and Fig. 3. Figure 3d shows the … See more UV-visible absorption spectroscopy (UV-vis) was used to explore the optical properties of TiO2 and CuSA-TiO2. The pristine TiO2 shows an absorption edge starting from 380 nm, … See more To examine the real chemical states of the photocatalysts during the photocatalytic reaction, in-situ x-ray photoelectron spectroscopy (XPS) spectra of CuSA-TiO2 before and during the reaction were monitored (Fig. 3b). … See more how do i know if microsoft edge is up to date